BNAI ZION SCIENTIST DIVISION

in cooperation with

COOPER UNION SCHOOL OF ENGINEERING  

   

Principles of Instrumental Analysis: Spectroscopy

 

Course layout:

The class will consist of lectures on these various topics, emphasizing both the theoretical and practical aspects of the various techniques. Students will be taught common spectroscopic techniques: their theory, scope and limitations, and applications.

    Text:      Skoog, D. A., Holler, F. J., and Crouch, S. R., Principles of Instrumental Analysis, 6th ed., Brooks Cole, 2006

Recommended additional material:

              This course will assume a basic understanding/knowledge of general and organic chemistry. Here are some supplementary textbooks that may be helpful:

Ebbing, General Chemistry

Solomons, Organic Chemistry

Skoog, D. A., West, D. M., Holler, F. J., and Crouch, S. R., Fundamentals of Analytical Chemistry, 8th ed., Brooks Cole, 2003

Harris, D. C., Quantitative Chemical Analysis, 7th ed., W. H. Freeman, 2007

             

Tentative Schedule:

Week

Topic

Chapter(s)

1

Introduction: Fundamentals of Analytical Chemistry, Instrumental Analysis and Quality Control

Harris, 4 and 5

2

Gas Chromatography-Mass Spectrometry (GC-MS)

Experiment: Analyzing Fragmentaton Patterns of Organic Compounds (C,H), (C,H,O) and (C,H,N)

Skoog, 20

3

Ultraviolet (UV) and Fluorescence Spectroscopies

Experiment: Determining Caffeine Concentration of an Unknown Solution Using UV Spectroscopy

Experiment: Determining Aspirin Concentration of an Unknown Solution Using Fluorescence Spectroscopy

Skoog, 13 14 and 15

4

Infrared (IR) and Raman Spectroscopies

Experiment: Determining Gluocse and Sucrose Concentrations of Unknown Solutions Using Attenuated Total Reflectance (ATR) FT-IR and Raman Spectroscopies

Skoog, 16 17 and 18

5

Nuclear Magnetic Resonance (NMR) and Electron Paramagnetic Resonance (EPR) Spectroscopies

Experiment: Identifying the Molecular Structure of an Organic Compound Using NMR Spectroscopy

Skoog, 19

6

Atomic Absorption (AA) Spectroscopy

Experiment: Determining the Lead Concentration of an Unknown Solution Using Graphite Furnace Atomic Absorption Spectroscopy

Skoog, 9

   

Instructor: Prof. Ruben Savizsky

Email: rsavizky@cooper.edu

Class Hours:      Saturday 12 pm - 4 pm